TEM FINAL!!

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    23-Aug-2014

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1 3 311031 1 ' MET: 3311133113 : : 301035053. 333300553. 153005503. 13' : 2 : .3 . 3 MET- , , . : ( ) . , : . TFF , , , , : FD - FB .mn51.074.9 = uAd, mn22.011.3 = eFd .]12-1[ . C008 - C005- . . . 3 : .1 . MET -. , , MET . -dcc . ( ]3], [1], [0[ . , ). . ( ) " - " MET - - , ( nis / 16.0 = ): 0( ]1], [0[). , (, , ) 5 : . , . ]1], [0[. : . " . " . D.A.S. . , . -d ][ ; -][ (: : )3( ]1], [0[). - ; , . . ) 1 ( . ( ), ]1], [0[ . ]3], [1], [0[ :MET- , . . FB FD ( ) ) AS- ( . . . . -, : 4 . " , , . , . . . . " , , . . , , . ). FB " " ( ).FD " " (, MET :METS . " ]5[ ( ). . :SDE . , ]5], [0[ . . 5 : .1 INACET 02T , MET : MET- . 6BaL ("") . IEF " . , . 9-50-3-50]rrot[. VeK[002[ - :, - 3O2lA) (uA) (eF ( .0 ). noitisoped maeb nortcele : ]1], [0[ . ; FD, FB: ; , . - C005 - ) 2OiT ( .1 .C008: gninipsortcelE : () , . "" ' . ]0[ . MET- ; . FD ,FB: ; 6 : .4 : 0 MET .0 ()- DAS .0.0 : FB .1.0 )04-1-( )041( )1-13( )210( )11-3-( )2-1-0( ]12-1[ )3O2lA-( eF uA )2-31( )23-1-( 7 : FD .3.0 , .5.0 .0.0 )3O2lA-( eF uA )3O2lA-( eF uA 8 0.0 TFF .1.0 .3.0 ):FD( 3.0 -) FB( 1.0, .3.0 ]mn] ]mn] 33.9 33.3 06.9 33.3 06.9 08.2 06.9 70.3 33.9 02.3 33.9 39.2 74.9 11.3 : 51.0 22.0 : mc5.7=mn01 : 22.011.3 = eFd): mn ( 51.074.9 = uAd): mn ( )3O2lA-( eF uA 9 553 C 20iT .1 C0005 5 . . 20iT .0.1 . , 20iT .1.1 ., 20iT .3.1 2 1 1 1 2 2 01 , .20iT .5.1 -( .0.5.1 ).5 ecapsd .1.5.1 0 METS .0.1 ]mc[R2 ][clacd ][yhtd }l,k,h{ ]%[rorrE 8 5.3 5.3 }101{ 6.0 3.00 4.2 4.2 }400{ 3.0 4.61 7.1 7.1 }501{ 4.0 6.81 5.1 5.1 }312{ 8.0 ]mc[R2 ][clacd ][yhtd }l,k,h{ ]%[rorrE 7.9 4.3 5.3 }101{ 7.0 9.11 4.2 4.2 }400{ 1.1 4.41 9.1 9.1 }200{ 8.2 6.61 7.1 7.1 }501{ 8.0 2 1 FD FB 11 SDE .1.1 .0.1 21 : .0 : 0 .0 , . : .0.0, " )3.0( FD-) 1.0( FB " : . . :mn51.074.9 = uAd, mn22.011.3 = eFd . . . . . . ) ( , . : .1.0-. " DAS 0.0 . 0 . 3O2lA- SDPCJ ] . 12-1 [ tff . 5.0-1.0 tff . 59 . 59 ).1-13( : .3.0 : FD/FB / .0.3.0 5.0 . FD 3.0 FB 1.0 . . ( ) , ( ) " . . , , FB- , FD-. . . FB 1.0 . (, ) , . 31 , . . - . FD 3.0 1.0 . ). , ( 5.0 . - . , " . , : .1.3.0 . 0.0 TFF 1.0 . 0.0 . TFF ). sdor-liar ( "". 0.0 (). ) 0.0 ( TFF" . , ).1-13 ( 59 , . . .-) mn2 ( . : 2OiT .1 . 0.1 .0.1 . , " . , . . - 1.1 .1.1 , . . . , . , " - 3.1 .3.1 ).5.1 - ( 41 . , , . " , , . . ).3.1 ( . mn41=D mn03=D . 5.1 .5.1 , . 1.5.1 0.5.1 DAS " DAS . . , , . , ecapsd . esatanA , . , R2 " . .0.1, C005 C008 : , , . . " , . . , . . . . . , " , . , " . DAS . 51 SDE 1.1 .1.1 , . , . . dirg " SDE .. , , . . , 61 : .6 " , MET- . ( : ), , . . , . mn51.074.9 = uAd, mn22.011.3 = eFd . .]12-1[ . - , . " .esatanA MET " . - 17 1. : 0. Microstructural Characterization of Materials, David Brandon and Wayne D. Kaplan 1. 3 TEM " ,0." 3. http://en.wikipedia.org/wiki/Transmission_electron_microscopy 5. http://en.wikipedia.org/wiki/Scanning_transmission_electron_microscope 0. http://en.wikipedia.org/wiki/Electrospinning 1. JCPDS: -Al2O3 , TiO2. 18 3. 3 :JCPDS Anatase TiO2. 1: JCPDS Rutile TiO2. 91 3O2lA- SDPCJ :1 :4 L 2=ecapsdR2 . " L :: 0 (). . 3 SDPCJ R2. xamd/id = iR2/nimR2 " : d , 1) 105. ( 1222 1 1 2 2 1 2 1 2 12 22 2 2 2 2 22 22 2 2 2 2 1 1 1 13) (5.0soc43 3() (4 4al l k h k h k k hhca al k h k h l k h k hc c ) 5( . . 1

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